Calorimetry Concepts: How To
The below links cover a wide range of concepts that aim to teach you how to preform calorimetry using our calorimeters and associated technology
How to Adjust the Sample Mass for Different CV
The CAL3K needs to operate at the calibration conditions. Since it is measuring the temperature rise during the burning…
Read MoreHow to Handle Calibrations
A calibration is needed for every vessel and every operating condition. During a calibration many variables are saved, such as Ambient temperature, Heat capacity and how the vessel ‘reacts’...
Read MoreHow to Handle Difficult Samples
A difficult sample is one which causes grief. This is indicated when: The results are not consistent, The sample doesn’t ignite, The CAL3K..
Read MoreHow To Measure Low CV Samples
Low Calorific Values are measured when substances are tested for their energy contribution to a fire. This is required for airline..
Read MoreHow To Measure Powdery Samples
Powdery substances like Saw dust, flour, or Benzoic Acid powder will burn violently and ‘scatter’ part of the sample material...
Read MoreHow To Measure Powerful Samples
Powerful samples have a very high CV. The highest (nongaseous) is Kerosene at 48Kj/g. All the fuels are not far behind and fat is 37Kj/g. Note that Dynamite is not powerful but fast burning...
Read MoreHow To Measure Samples With High Moisture
The moisture content of a sample affects the result directly: a 1% difference in moisture will make a 1% difference in the result. The CAL3K ...
Read MoreHow To Measure Spiking Accessories
Spiking is the method where a known substance (The Spike) is burned together with the unknown sample to....
Read MoreHow To Measure The CV Of Cotton Thread
This is a difficult operation because the cotton cannot be ignited without the firing wire (energy). Before the cotton can be measured perform...
Read MoreHow To Measure the CV of Gelatin Capsules
The gelatin capsule (part number 3K-4-068) is used for powdery substances and during spiking...
Read MoreHow To Measure the Firing Energy for Different Wire
The sample is ignited by sending a high current through the firing wire which heats the wire to approx. 800 degrees °C. This intern...
Read MoreHow To Measure Volatile Samples
Volatile samples are alcohols and acetone. Some fuels have a volatile component as well. If the sample evaporates between the weight-in and the ignition then the evaporation must be stopped...
Read MoreHow to Check a Misfire
The CAL3K measures, in broad terms, the temperature rise in the vessel when a sample is burned. The sample is ignited (fired), and when it doesn’t ignite then we call it a ‘misfire’...
Read MoreHHV and LHV Calorific Values
A calorimeter measures the High Heating Value (HHV) because the combustion is contained in a closed environment…